Electrochemical hydrogenation of a benzannulated pyridine to a dihydropyridine in acidic solution.
CHEMICAL COMMUNICATIONS(2018)
摘要
The electrochemistry of pyridines in acidic solution is dominated by a 'weak acid' reduction on the cyclic voltammetry timescale. Here we show that electrochemical hydrogenation of a benzannulated pyridine, phenanthridine (1), to the biomimetic hydride donor 1,2-dihydrophenanthridine (1-H-2) can occur selectively at glassy carbon electrodes over longer timescales of potentiostatic electrolysis.
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关键词
electrochemical hydrogenation,dihydropyridine
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