ChemInform Abstract: Large‐Scale and Facile Preparation of Pure Ammonia Borane Through Displacement Reactions.

Xuenian Chen,Xiaoguang Bao,Beau Billet,Sheldon G Shore,Jicheng Zhao

Cheminform（2013）

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摘要

Pure NH3BH3 is prepared at the 100 g scale by displacement reactions of either NH3 and Me2S·BH3 with 94% yield, or NH3 and Ph-NMe2·BH3 with 91% yield, with both reactions performed in toluene at room temperature.

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