Synthesis of (±)‐Bakuchiol via a Pot‐Economy Approach

Mengyuan Huang,Long Chen,Ruoxi Li,Xueshun Jia,Ran Hong

CHINESE JOURNAL OF CHEMISTRY（2014）

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摘要

A rapid synthetic route toward (+/-)-Bakuchiol is presented in 29% overall yield. After the sole all-carbon quaternary carbon center is created via allylboration of 2-aryl acetaldehyde, a "Pot-Economy" approach including mesylation, elimination, and desilylation was realized in the presence of tBuOK under ambient temperature to provide (+/-)-Bakuchiol.

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关键词

allylboration,bukuchiol,meroterpenoid,pot-economy,quaternary carbon

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