A simple and selective method for determination of phthalate biomarkers in vegetable samples by high pressure liquid chromatography–electrospray ionization-tandem mass spectrometry

Xi Zhou,Kunyan Cui,Feng Zeng, Shoucong Li,Zunxiang Zeng

Food Chemistry（2016）

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摘要

•Clean-up techniques of phthalate monoesters from vegetable samples were optimized.•Sample preparation based on ultrasonic extraction followed by liquid–liquid extraction.•Quantification of phthalate monoesters in vegetable samples by LC–MS/MS was developed.

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关键词

Phthalate monoester metabolites,Ultrasonic extraction,Liquid–liquid extraction,Solid-phase extraction,Vegetable,High pressure liquid chromatography–electrospray ionisation-tandem mass spectrometry

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