Reaction Of Ph2p(Ch2)(N)Pph2 (N=1, 3, 5) With Elemental Tellurium And Comparison With Members Of Even-Numbered Series

Lukas Jeremias,Michal Babiak,Vclav Kubat,Maria Jose Calhorda,Zdenek Travnicek,Josef Novosad

INORGANICA CHIMICA ACTA（2016）

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摘要

The oxidation of Ph2P(CH2)(n)PPh2 (n = 1, 3, 5) by tellurium powder was studied. The prepared compounds Ph2P(Te)(CH2)(n)P(Te)Ph-2 (1, n = 3; 2, n = 5) were characterized by P-31 and Te-125 NMR spectroscopy, elemental analysis, FTIR spectroscopy and for 2 by single-crystal X-ray analysis. (C) 2016 Elsevier B.V. All rights reserved.

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关键词

Bis(diphenylphosphino)alkane telluride,X-ray analysis,Multinuclear NMR spectroscopy,Te-transfer

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