Synthesis, characterization and analysis of the acrylamide- and glycidamide-glutathione conjugates

Yu-Syuan Luo,Tai-Ying Long,Li-Ching Shen,Shou-Ling Huang,Su-Yin Chiang,Kuen-Yuh Wu

Chemico-Biological Interactions（2015）

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摘要

•Synthesized and characterized AA- and GA-GSH conjugates.•Developed a robust LC–ESI-MS/MS method to analyze AA- and GA-GSH conjugates.•Successfully determined the AA-GSH, GA2-GSH and GA3-GSH in rat blood.•Analysis of GSH conjugates provides direct evidence on AA and GA detoxication.

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关键词

AA,AAMA,COSY,EH,GA,GAMA,GSH,GST,HESI,HMBC,HSQC,LOD,LOQ,MAs

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