Tutorial review on validation of liquid chromatography-mass spectrometry methods: Part I.

Anneli Kruve,Riin Rebane,Karin Kipper,Maarja-Liisa Oldekop,Hanno Evard,Koit Herodes,Pekka Ravio,Ivo Leito

Analytica Chimica Acta（2015）

引用 278|浏览20

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摘要

•The status of validation of LC–MS methods is comprehensively reviewed.•Clarity is brought into validation-related terminology.•Recommendations on difficult validation-related issues in LC–MS are given.

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关键词

CRM,CV,EMA/EMEA,ESI,FDA,ICH,ILC,ILIS,IS,IUPAC,LC–MS,LLoQ,LoD,LoF,LoQ,ME,MU,PE,r,R,r2,RSD,s,SLV,ST%,ULoQ,VIM

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