20,23,26,29,32,35,38,41-Octaoxa-5,9,13-triazapentacyclo[15.14.10.-1 3,30.1 7,11.1 15,19]tetratetraconta-1,3(42),7,9, 11(44),15(43),16,18,30-nonaene-6,12-dione acetone monosolvate

Acta Crystallographica Section E: Structure Reports Online(2012)

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摘要
In the crystal structure of the title compound, C 33H 39N 3O 10-C 3H 6O, the acetone molecule is encapsulated into the cavity of the cryptand and fixed by two N-H··· O and one C-H··· O hydrogen bond. C-H···O and C-H···N interactions link neighbouring cryptands. The dihedral angles between the pyridine ring and the benzene rings are 86.47(17) and 85.53(13)°.
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data-to-parameter ratio = 8.0,mean σ(c-c) = 0.008 å,r factor = 0.056,single-crystal x-ray study,t = 298 k,wr factor = 0.172
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