Unusual oxidation behaviour of a propargylic alcohol

Michael J. Porter,Nicola J. White,Garnet E. Howells,David D.P. Laffan

Tetrahedron Letters（2004）

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摘要

Attempts to convert a propargylic alcohol bearing an imidazolone substituent to the corresponding aldehyde under Parikh–Doering conditions gave an α,β-unsaturated-β-methylsulfanyl aldehyde, which cyclised under mildly acidic conditions.

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关键词

Agelastatin,Oroidin,Imidazolone,Parikh–Doering oxidation,Conjugate addition,Nazarov

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