ChemInform Abstract: Formation and Crystal Structure of an Unexpected Inclusion Complex of a Metal-Free Phthalocyanine and Oxalic Acid.

Wei Liu,Chi-Hang Lee,Hung-Wing Li,Chi-Keung Lam, Jinzhi Wang,Thomas C. W. Mak,Dennis K. P. Ng

Cheminform（2010）

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摘要

Treatment of 3-(2,4-dimethyl-3-pentyloxy)phthalonitrile (2) with CeCl3 in the presence of 1,8-diazabicyclo[5.4.0]undec-7-ene (DBU) in n-pentanol gives the corresponding metal-free phthalocyanine 3, which unexpectedly traps the oxalic acid in the crystal lattice forming a 1∶1 inclusion complex.

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crystal structure

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