Pilot plant synthesis of methacrylate copolymer precursors to nonlinear optical materials
JOURNAL OF APPLIED POLYMER SCIENCE(1990)
摘要
The copolymerization of method methacrylate with methacrylates containing anilino side chains was investigated. Azobis (isobutyronitrile) was a better initiator than benzoyl peroxide. Continuous feed of initiator was advantageous compared to adding the initiator all at once. The reaction was scaled up using a 10-L reactor, ultimately yielding hundreds of grams of the desired copolymers, which are valuable precursors to polymeric dyes used in nonlinear optical studies
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