High yield synthesis of the parent C-unsubstituted calix[4]resorcinarene octamethyl ether

Olusegun M. Falana,Emile Al-Farhan,Philip M. Keehn,Robert Stevenson

TETRAHEDRON LETTERS（1994）

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摘要

Treatment of 2,4-dimethoxybenzyl alcohol with trifluoroacetic acid (TFA, 5% in CHCl3) affords, in almost quantitative yield calix[4]resorcinarene octamethyl ether, which on demethylation and acetylation yields the derived octa-acetate.

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