Samarium iodide mediated methylation: an alternative to grignard labeling

JOURNAL OF LABELLED COMPOUNDS & RADIOPHARMACEUTICALS（2000）

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摘要

Samarium iodide in THF/HMPA has been used to methylate various aldehydes and ketones in moderate to good yield. Reaction is complete within two minutes. Labeling using methyl-[C-14] iodide has been successful and is thus an alternative to labeling via a methyl Grignard derived from methyl-[C-14] iodide.

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关键词

samarium iodide,methyl iodide,Grignard,Barbier Reaction

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