Synthesis of Melithasterol A, a 5α,6α-Epoxy-7α-hydroxy Δ⁸-Steroid^†

P. Ramesh,V. L. Niranjan Reddy,N. Srinivasa Reddy,Y. Venkateswarlu

JOURNAL OF NATURAL PRODUCTS（2000）

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摘要

A short, first synthesis of melithasterol A (3) utilizing microwave irradiation-induced isomerization of 5 alpha ,8 alpha -epidioxy steroid (1) as the key step has been achieved in 80% yield.

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Synthesis of Melithasterol A, a 5α,6α-Epoxy-7α-hydroxy Δ8-Steroid†

Synthesis of Melithasterol A, a 5α,6α-Epoxy-7α-hydroxy Δ⁸-Steroid^†